Reference of 5888-51-7, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 5888-51-7, name is 4-Ethyl-1,2-dimethoxybenzene, This compound has unique chemical properties. The synthetic route is as follows.
General procedure: A sealed tube equipped with a magnetic stirring bar was charged with ethylarene (1, 1.0 mmol), aq NH3 (2, 25% aq solution,10.0 mmol), I2 (1.1 mmol), and TBHP (6.0 mmol, 70% aq solution) at r.t. The resulting mixture was heated to 100 C for 3.0 h. After completion of the reaction (monitored by TLC), sat.Na2S2O3 solution (10 mL) was added to the reaction mixture,and it was extracted with EtOAc (2 ¡Á 20 mL). The organic layer was washed with brine solution (20 mL), dried over anhydrous Na2SO4 and concentrated under reduced pressure. The residue was purified by column chromatography on 100-200 mesh silica gel using EtOAc-n-hexane (1:2) as the eluent to obtain the corresponding benzamide 3.
The chemical industry reduces the impact on the environment during synthesis 4-Ethyl-1,2-dimethoxybenzene. I believe this compound will play a more active role in future production and life.
Article; Vadagaonkar, Kamlesh S.; Kalmode, Hanuman P.; Prakash, Sattey; Chaskar, Atul C.; Synlett; vol. 26; 12; (2015); p. 1677 – 1682;,
Ether – Wikipedia,
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