Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 621-23-8, name is 1,3,5-Trimethoxybenzene, This compound has unique chemical properties. The synthetic route is as follows., Application In Synthesis of 1,3,5-Trimethoxybenzene
In the reactor, 100 mg of 1,3,5-trimethoxybenzene and 20 mg of boron-nitrogen carbon photocatalyst were added.100 mg of ammonium chloride is an amine source, 3 ml of dimethyl sulfoxide and 1.2 equivalents of cesium fluoride (regulating the pH of the initial reaction solution to 8-10),The reaction was stirred with light at room temperature for 48 h in an oxygen atmosphere, and then extracted with ethyl acetate.The combined organic layers were dried, filtered and evaporatedThe column chromatography eluate used was a petroleum ether: ethyl acetate mixed solvent in a volume ratio of 10:1.The yield was 41%.
According to the analysis of related databases, 621-23-8, the application of this compound in the production field has become more and more popular.
Patent; Fuzhou University; Wang Xinchen; Zheng Meifang; Yuan Tao; Shi Jiale; (7 pag.)CN108546233; (2018); A;,
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