Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 3586-14-9, name is 1-Methyl-3-phenoxybenzene, A new synthetic method of this compound is introduced below., COA of Formula: C13H12O
EXAMPLE 1 Into a 200 ml four necked flask equipped with a distillation column, 36.9 g (0.2 mole) of m-phenoxytoluene and 1.0 g of powdery activated carbon were charged and heated at 180 C. while stirring and then, 71.1 g of 1,2-dibromotrichloroethane (0.24 mole) was added dropwise for 30 minutes and the reaction was continued at the temperature for 3 hours. After the reaction, the reaction mixture was analyzed by a gas chromatography, 1,2-dibromotrichloroethane disappeared, and the production of 27.5 g of m-phenoxybenzyl bromide and 20.2 g of m-phenoxybenzylidene dibromide were found.
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; Toyo Soda Manufacturing Co., Ltd.; US4393246; (1983); A;,
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