Adding a certain compound to certain chemical reactions, such as: 645-36-3, name is 2,2-Diethoxyethanamine, belongs to ethers-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 645-36-3, Application In Synthesis of 2,2-Diethoxyethanamine
A solution of 1-NAPHTHALENYLTHIOISOCYANATE (893 mg, 4.82 MMOL) and 2- AMINOACETALDEHYDE DIETHYL ACETAL (0.70 mL, 4.85 MMOL) IN TOLUENE (10 mL) was stirred at room temperature for 1 h. Aqueous 12 N HCI solution (0.2 mL) was added and the mixture was heated at 110 C for 3 h and then stirred at room temperature for 16 h. The mixture was concentrated under reduced pressure. The residue was triturated with hot EtOAc to give the title compound (608 mg, 56% yield).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2,2-Diethoxyethanamine, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; BOEHRINGER INGELHEIM INTERNATIONAL GMBH; WO2004/50643; (2004); A2;,
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