In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 111-95-5, name is Bis(2-methoxyethyl)amine belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. 111-95-5
In a 100 ml eggplant type flask, 3.6 ml (25 mmol) of bis (2-methoxyethyl) amine,3.2 g (25 mmol) of phloroglucinol and 30 ml of THF were added and stirred. After 48 hours,The reaction was confirmed by TLC (SiO 2, developing solvent hexane: acetone = 1: 1), followed by extraction with chloroform, and the solvent was distilled off under reduced pressure to obtain a black viscous substance (yield 5.1 g, yield 86 %).
The synthetic route of 111-95-5 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Satoru: Yamagata University; Kido Junji; Sasabe Hisa Hiroshi; Sasaki Isamu; (15 pag.)JP6281975; (2018); B2;,
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