Adding some certain compound to certain chemical reactions, such as: 60792-79-2, name is 2,2′-Oxybis(ethylamine) dihydrochloride, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 60792-79-2. 60792-79-2
EXAMPLE 31 2,2′-[Oxybis(ethanediyldiimino)]bis(1,2-diphenylethanol). A mixture of trans-stilbene oxide (2.21 g, 0.0113 mol), 2-(2-aminoethoxy)ethylamine dihydrochloride (1 g, 0.00565 mol) and sodium bicarbonate (0.95 g, 0.0113 mol) were stirred together in n-butanol (10 mL) and heated on a steam bath for 16 hours. Upon cooling a solid formed. The mixture was triturated with methanol (25 mL) and the mixture then diluted with water (200 mL). The solid was collected and dried under ambient conditions on absorbent paper for 2 hours. The solid still had a strong odor of 1-butanol. The solid was heated in boiling toluene (50 mL) and isooctane (25 mL) added to the boiling solution. The organic layer was decanted from a small amount of a denser second layer, presumably water. Upon cooling, the product crystallized from the toluene-isooctane mixture. The solid was collected and dried under ambient conditions for 18 hours to obtain 2.05 g (92% yield); mp 161-164 C. Analysis: Calculated for C32 H36 N2 O3: C, 77.39; H, 7.31; N, 5.64 Found: C, 77.40; H, 7.32; N, 5.77
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 2,2′-Oxybis(ethylamine) dihydrochloride.
Reference:
Patent; A. H. Robins Company, Incorporated; US5171753; (1992); A;,
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