A new synthetic route of 2752-17-2

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 2,2′-Oxydiethanamine.

Adding some certain compound to certain chemical reactions, such as: 2752-17-2, name is 2,2′-Oxydiethanamine, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 2752-17-2. 2752-17-2

Cyanuric chloride (2.05 g, 11 mmol, 2 eq)Was dissolved in acetonitrile (25 mL)Cooled to 0 C, 2,2′-oxybis (ethylamine) (0.56 mL, 5.4 mmol, 1 eq)And NaHCO3 (1.83 g, 22 mmol, 4 eq)Followed by addition of the above solution,0 reaction 2h,The reaction is completed.Vacuum steaming solvent,Dissolved in CH2Cl2,Filter out insoluble matter,The filtrate was dried over anhydrous magnesium sulfate,The solvent is evaporated,To give the compound 2,2′-oxobis (ethylamine) -4,4 ‘, 6,6′-tetrachloro-1,1’, 3,3 ‘, 5,5′-briquine (ECl2).

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 2,2’-Oxydiethanamine.

Reference:
Patent; University of Science and Technology of China; Ma Mingming; Zhang Ning; Yan Ziqiang; (32 pag.)CN107235925; (2017); A;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem