The origin of a common compound about 3-Ethynylanisole

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Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 768-70-7, name is 3-Ethynylanisole, This compound has unique chemical properties. The synthetic route is as follows., 768-70-7

At room temperature, FTA-Au(I)catalyst (2 mol%), AgOTf (5 mol%) was added to a stirring solution of 6a (1.0 mmol) in HOAc/H2O(10:1, 4 mL), then the reaction mixture was heated to 100 oC andstirred overnight (12 h). After the reaction completed, the solvent was removedunder reduced pressure and the residue was purified by flash chromatography onsilica gel (ethyl acetate/hexane = 1 : 80, V/V) to give the title compound 7a in 89% yield as light yellow oil.

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Reference:
Article; Yao, Wei; Zhang, Yilin; Xu, Xiaqing; Yang, Yongchun; Zeng, Wei; Wang, Dawei; Journal of Organometallic Chemistry; vol. 901; (2019);,
Ether – Wikipedia,
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