Reference of 6346-09-4, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6346-09-4, name is 4,4-Diethoxybutan-1-amine, This compound has unique chemical properties. The synthetic route is as follows.
General procedure: Under an argon atmosphere, a solution is prepared containing amino acetal (1.2 mmol) and triethylamine (2.0 mmol) in dry chloroform (10 mL). The mixture is cooled to 0 C and a solution of the acid chloride (1 mmol, in 5 mL of CHCl3) is added slowly with stirring. The mixture is allowed to warm to room temperature for 3 h. Following this reaction period, the mixture is extracted twice with chloroform. The organic extracts are then washed with 1 M HCl, with water, and twice with brine solution. After drying over anhydrous sodium sulphate, the organic solvent is removed by reduced pressure and the crude product is subject to column chromatography (SiO2, hexanes:ethyl acetate).
The chemical industry reduces the impact on the environment during synthesis 4,4-Diethoxybutan-1-amine. I believe this compound will play a more active role in future production and life.
Reference:
Article; Kennedy, Sean; Kethe, Anila; Qarah, Ahmad; Klumpp, Douglas A.; Tetrahedron Letters; vol. 59; 20; (2018); p. 1932 – 1935;,
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