Adding a certain compound to certain chemical reactions, such as: 2398-37-0, name is 1-Bromo-3-methoxybenzene, belongs to ethers-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 2398-37-0, HPLC of Formula: C7H7BrO
General procedure: The typical procedure is as follows. Oven dried Schlenk tube was equipped with stirrer bar, was charged with aryl halides (1 mmol), aryl phenylboronic acid (1.2 mmol), K2CO3 (2 mmol) and catalyst2 (3 mol %) in1:1 mixture of DMF/H2O medium. The reaction mixture was stirred in an oil bath at 100C in the presence of air. After completion of the reaction, the reaction mixture was then cooled to room temperature and diluted with Et2O/H2O (1:1, 20 mL). The organic layer was alienated and dried with anhydrous MgSO4. The product was filtered and dried under vacuum. The resulting crude compound was purified by column chromatography on silica gel to afford the corresponding products.
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Reference:
Article; Nirmala, Muthukumaran; Arruri, Sathyanarayana; Vaddamanu, Moulali; Karupnaswamy, Ramesh; Mannarsamy, Maruthupandi; Adinarayana, Mannem; Ganesan, Prabusankar; Polyhedron; vol. 158; (2019); p. 125 – 134;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem