Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 1706-12-3, name is 1-Methyl-4-phenoxybenzene, This compound has unique chemical properties. The synthetic route is as follows., name: 1-Methyl-4-phenoxybenzene
A moderate stirrer was placed in a dry reaction tube (20 ml), palladium hydroxide/carbon (30 mol%), NaBH4 (1.5 equivalents) was added, and then the reaction tube was evacuated, filled with argon gas, and repeatedly replaced three times. A solution of 4-methyldiphenyl ether (0.2 mmol) and tetrahydropyrrole (0.7 mmol) dissolved in a solvent was slowly added to the reaction tube with a syringe under an argon atmosphere, and 10 uL was added to the reaction tube using a micro-injector. Water, then 1 mL of air was added to the reaction tube with a syringe, and the reaction tube was placed in an oil bath at 160 C to heat and stir the reaction. After 24 hours, the reaction was stopped, the reaction tube was taken out from the oil bath, cooled to room temperature, diluted with ethyl acetate, and then filtered over Celite, and the yield of benzene in the gas phase was 74%. The filtrate was concentrated and separated by an activated thin layer chromatography chromatography plate (eluent: n-hexane/ethyl acetate = 100/1).The final product was obtained in 5g and 4g. Product 5g (yield: 62%)
According to the analysis of related databases, 1706-12-3, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Lanzhou University; Zeng Huiying; Cao Dawei; Li Chaojun; (19 pag.)CN109553592; (2019); A;,
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