Continuously updated synthesis method about 2930-05-4

Statistics shows that 2-((Benzyloxy)methyl)oxirane is playing an increasingly important role. we look forward to future research findings about 2930-05-4.

Related Products of 2930-05-4, These common heterocyclic compound, 2930-05-4, name is 2-((Benzyloxy)methyl)oxirane, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

General procedure: IL/DFNS NPs (5mg) and epoxide derivatives (1mmol) werecharged into the reactor vessel without using any co-solvent. The reactor vessel was placed under a constant pressure ofcarbon dioxide and then heated to 70C for 2h. Then thereactor was cooled to ambient temperature, and the resultingmixture was transferred to a 50mL round bottom flask.Upon completion, the progress of the reaction was monitoredby TLC when the reaction was completed, EtOH wasadded to the reaction mixture and the KCC-1/IL/HPW NPswas separated by filteration. Then the solvent was removedfrom solution under reduced pressure and the resulting productpurifed by recrystallization using n-hexane/ethyl acetate.

Statistics shows that 2-((Benzyloxy)methyl)oxirane is playing an increasingly important role. we look forward to future research findings about 2930-05-4.

Reference:
Article; Zhang, Pu; Zhiani, Rahele; Catalysis Letters; vol. 150; 8; (2020); p. 2254 – 2266;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem