Related Products of 51344-14-0, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 51344-14-0, name is N,N-Dimethyl-2-(p-tolyloxy)ethanamine belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
58.9 g (0.495 mol) of potassium bromide,Hydrogen peroxide 60 ml,Water 60 ml and 150 ml of chloroform were added to a liter of three bottles,Drop under ice bath32 ml concentrated sulfuric acid,Drop finished, remove the ice bath,Add 4- (2-dimethylaminoethoxy) toluene134 g (0.75 mol),The reaction solution was refluxed under light for 2 h,After completion of the reaction, the organic layer was separated, dried over anhydrous sodium sulfate, And the crude product was distilled under reduced pressure to give 185 g of a pale yellow liquid in a yield of 96%.
The synthetic route of N,N-Dimethyl-2-(p-tolyloxy)ethanamine has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Anhui Cheng Lian Pharmaceutical Technology Co., Ltd.; Liu Hui; (5 pag.)CN106748821; (2017); A;,
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