In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 701-56-4, name is 4-Methoxy-N,N-dimethylaniline belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. Safety of 4-Methoxy-N,N-dimethylaniline
The second step, 28.2 grams of oil,200 ml of toluene,27 grams of anhydrous aluminum chloride was added to a 500 ml three-neck bottle.The temperature was refluxed for 6 hours in an oil bath.Cool down to 80 C,Slowly add 100 ml of saturated sodium bicarbonate solution.Produce a solid,Continue to stir for 10 minutes.Filter out the insoluble matter while hot,After filtration, hot liquid separation,Add 50 ml of water to the toluene.Warmed up to 80 C together,Stir for 10 minutes,Liquid separation,The toluene phase is dried,Then use an oil pump to decompress and distill.Curing to obtain 20.8 grams of product,99.8% purity,The yield was 81%.
The synthetic route of 701-56-4 has been constantly updated, and we look forward to future research findings.