Adding a certain compound to certain chemical reactions, such as: 2688-84-8, name is 2-Phenoxyaniline, belongs to ethers-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 2688-84-8, HPLC of Formula: C12H11NO
In a dry 25 mL Schlenk reaction tube, 55.6 mg of 2-phenoxyaniline was added.71 mg of 4-methylstyrene, 38.4 mg of sulfur, 35 mg of potassium fluoride and 1.5 mL of dimethyl sulfoxide.Stir at 100 C for 24 hours under nitrogen.After completion of the reaction, the mixture was cooled to room temperature, and the insoluble material was removed by filtration, washed with water and ethyl acetate.Directly through the silica gel column (the ratio of ethyl acetate to petroleum ether is 1:50-1:3),The product was obtained in 88.0 mg, yield 92%.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-Phenoxyaniline, other downstream synthetic routes, hurry up and to see.