Adding a certain compound to certain chemical reactions, such as: 10075-63-5, name is 1,5-Dimethoxynaphthalene, belongs to ethers-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 10075-63-5, Application In Synthesis of 1,5-Dimethoxynaphthalene
To a suspensionof 1,5-dimethoxy-naphthalene (3.76 g, 20 mmol)in acetonitrile (50 mL) was added NBS (3.9 g,22 mmol) at room temperature. Upon stirring for 2 h,the precipitate was filtered off and washed with acetonitrile thus giving the crude product which wasrecrystallized from methanol and dried. Cyan-bluesolid, yield 88%. 1H NMR spectrum, delta, ppm: 3.85 s(3H), 3.90 s (3H), 6.74-7.13 m (2H), 7.29-7.48 m(1H), 7.54-7.87 m (2H). 13C NMR spectrum, delta, ppm:55.51, 55.72, 105.05, 107.99, 108.26, 114.92, 125.94,128.76, 132.23, 133.67, 154.69, 155.48.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1,5-Dimethoxynaphthalene, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Dong; Zhang; Huang; Meng; Li; Russian Journal of General Chemistry; vol. 87; 4; (2017); p. 837 – 841; Zh. Obshch. Khim.; vol. 87; 4; (2017); p. 837 – 841,5;,
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