In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 202865-58-5 as follows. category: ethers-buliding-blocks
Intermediate Example Int 10.22.011 -bromo-5-f luoro-2-methoxy-4-(methy Isu Ifany l)benzeneTo a stirred solution of sodium methanethiolate (0.47 g) in DMF (15 mL) at 0 C was added 1 -bromo-4,5-difluoro-2-methoxybenzene (1 .5 g). The mixture was stirred at r.t. for 2 h. Water was added and the mixture was extracted with ethyl acetate. The organic phase was washed with saturated sodium chloride solution, dried (sodium sulfate) and the solvent was removed in vacuum. Silica gel chromatography gave 1 .46 g of the title compound.
According to the analysis of related databases, 202865-58-5, the application of this compound in the production field has become more and more popular.
Reference:
Patent; BAYER INTELLECTUAL PROPERTY GMBH; SCHULZE, Volker; KOSEMUND, Dirk; WENGNER, Antje, Margret; SIEMEISTER, Gerhard; STOeCKIGT, Detlef; LIENAU, Philip; SCHIROK, Hartmut; BRIEM, Hans; WO2012/143329; (2012); A1;,
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