Related Products of 89282-70-2, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 89282-70-2, name is 2-Methoxy-2-methylpropan-1-amine belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
Preparation 3 Synthesis of N-(2-methoxy-2-methylpropyl) formamide Formic acid (19.2 g, 0.40 mol) and acetic anhydride (40.8 g, 0.40 mol) Were combined and heated to 45-50 C. for one hour and cooled to approximately 0 C. in an ice/acetone bath. A solution of 2-methoxy-2-methylpropyl-1-amine (36 g, 0.35 mol), precooled to approximately 0 C. in an ice/acetone bath was added slowly while keeping the temperature of the mixture below 12 C. After the addition was complete, the mixture was allowed to warm slowly to room temperature and was stirred at room temperature overnight. The solution was evaporated and the residue distilled at 97-107 C./1-2 mm Hg. to give 43.2 g (94%). NMR (CDCl3): delta 1.2 (s, 6H, CH3), 3.3 (m, 5H, CH3 O and CH2), 6.6 (b, 1H, NH), 8.2 (bs, 1H, HCO).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-Methoxy-2-methylpropan-1-amine, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; E. I. Du Pont de Nemours and Company; US4988827; (1991); A;,
Ether – Wikipedia,
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