Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 701-56-4, name is 4-Methoxy-N,N-dimethylaniline, This compound has unique chemical properties. The synthetic route is as follows., HPLC of Formula: C9H13NO
General procedure: A 25 mL round bottomed flask was charged with N,N-dialkyl-aniline (0.5 mmol), 2-naphthol (0.5 mmol) and acetonitrile (3 mL), followed by 10 mg of Ce-MCM-41 and TBHP (2 equiv.) via syringe. The mixture was heated to 60 C and stirred for 3 h in open air. After completion of the reaction, as judged by TLC, the solution was cooled and the catalyst was removed by filtration. The resulting crude mixture was gently evaporated under reduced pressure and purified by column chromatography using silica gel and a mixture of hexane and ethyl acetate as the eluent.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 701-56-4.
Reference:
Article; Akondi, Adinarayana Murthy; Trivedi, Rajiv; Sreedhar, Bojja; Kantam, Mannepalli Lakshmi; Bhargava, Suresh; Catalysis Today; vol. 198; 1; (2012); p. 35 – 44;,
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