Adding a certain compound to certain chemical reactions, such as: 2930-05-4, name is 2-((Benzyloxy)methyl)oxirane, belongs to ethers-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 2930-05-4, HPLC of Formula: C10H12O2
3-Benzyloxypropan-2-ol 16 To a suspension of lithium aluminum hydride (6.1 g, 0.16 mol) in ether (50 mL) at 25 C. was added a solution of glycidyl benzyl ether 15 (52.9 g, 0.32 mol) in 50 mL of ether (Step 13). The mixture was refluxed for 2 h and cooled to room temperature. A solution of 1N NaOH was added dropwise to the mixture and the precipitated metal salts were removed by filtration. The ether containing the product was washed with water (50 mL), dried (MgSO4) and the solvent removed by roto-evaporation. Distillation gave 43.3 g (82%) of 3-benzyoxypropan-2-ol; 16 bp 110-112 (5 mm). 1 H NMR (CDCl3) delta 1.13 (d, J=6.6 Hz, 3H, CH3), 2.5 (br s, 1H, OH), 3.28 (dd, 1H, OCH), 3.45 (dd, 1H, OCH), 4.0 (m, 1H, OCH), 4.55 (s, 2H, OCH2), 7.35 (s, 5H, phenyl).
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Reference:
Patent; Emory University; US5808146; (1998); A;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem