Continuously updated synthesis method about C9H13NO2

According to the analysis of related databases, 34967-24-3, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 34967-24-3, name is 3,5-Dimethoxybenzyl amine, This compound has unique chemical properties. The synthetic route is as follows., Formula: C9H13NO2

General procedure: Synthesis of (2R, 3R, 4S, 5R)-2-(6-(benzylamino)-9H-purin-9-yl)-5-(hydroxymethyl) tetrahydrofuran-3,4-diol, 2. In a 7 mL MW vessel, 6-chloropurinoriboside 3 (20 mg, 0.07 mmol), benzylamine 4 (7.5 mg,0.07 mmol, 7.7 muL) and triethylamine (7.08 mg, 0.07 mmol, 9.8 muL)were mixed. The solid mixture was stirred in CEM Explorer. MWMethod: T = 210 C, Power: 300 W, Hold Time: 1 min, P = 250 PSI,Power Max activated. After cooling, the solvent was removed in vacuoand the crude was dissolved in methanol and then purified on PTLC(DCM/MeOH 9:1) to afford compound 2 as white solid (24 mg, 94%).C17H20N5O4: 358.1510; Found 358.1515. Rt: 8.92 min.

According to the analysis of related databases, 34967-24-3, the application of this compound in the production field has become more and more popular.

Reference:
Article; Abate, Mario; Bifulco, Maurizio; Buonocore, Michela; Ciaglia, Elena; Covelli, Verdiana; D’Ursi, Anna Maria; Gazzerro, Patrizia; Grimaldi, Manuela; Randino, Rosario; Rodriquez, Manuela; Scrima, Mario; Stillitano, Ilaria; Tosco, Alessandra; Bioorganic Chemistry; (2020);,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem