In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 175278-09-8 as follows. Formula: C7H5BrF3NO
A solution of 8 g (31 mmol) of 4-bromo-2-trifluoromethoxyaniline and 4.2 g (37.5 mmol) of DABC (triethylenediamine) in 40 mL of toluene was slowly added dropwise 7 mL of carbon disulfide and the reaction was stirred at room temperature 8h. After the reaction, the reaction solution was suction filtered, and the filter cake was 3g of [4-bromo-2-trifluoromethoxyphenyl] dithioic acid with a yield of about 28%.
According to the analysis of related databases, 175278-09-8, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Xi’an Jiao Tong University; He, LangChong; Zhang, Jie; Pan, XiaoYan; Wang, Jinfeng; Su, Ping; Lu, Wen; Wang, Sicen; (17 pag.)CN105924385; (2016); A;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem