Related Products of 53087-13-1, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 53087-13-1, name is 1-(Benzyloxy)-3-bromobenzene, This compound has unique chemical properties. The synthetic route is as follows.
A mixture of 1-benzyloxy-2-bromobenzene (12.8 g, 48.7 mmol) and n-butyllithium (55 mmol) in THF (150 mL) was stirred for 20 min at -78 C, treated with tri-iso-propyl borate (34 mL, 147 mmol), stirred for 20 minutes at -78 C, then 30 minutes at ambient temperature. The mixture was reduced in volume by rotary evaporation, diluted with ethyl acetate washed sequentially with 1M HCl (twice), water, and brine, dried (MgSO4) and concentrated to provide a white solid which was triturated with hexanes to provide the title compound as a white powder (7.04 g). MS (DCI/NH3) m/e 246 (M+NH4)+.
The chemical industry reduces the impact on the environment during synthesis 1-(Benzyloxy)-3-bromobenzene. I believe this compound will play a more active role in future production and life.
Reference:
Patent; ABBOTT LABORATORIES; EP1080070; (2006); B1;,
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