In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 39021-83-5 as follows. Recommanded Product: 39021-83-5
A solution of 1,4-dimethoxy-2,3-dimethylbenzene 1 (1.00 g, 6.02 mmol) and N-bromosuccinimide (2.36 g, 13.2 mmol) in 1,1,1-trichloroethane (20 cm3) was heated under reflux for 1 h with visible irradiation. The mixture was filtered and the filtrate evaporated to leave the product 4 as a brown crystalline solid (0.55 g, 55%)
According to the analysis of related databases, 39021-83-5, the application of this compound in the production field has become more and more popular.
Reference:
Article; Aitken, R. Alan; Jethwa, Siddharth J.; Richardson, Neville V.; Slawin, Alexandra M.Z.; Tetrahedron Letters; vol. 57; 14; (2016); p. 1563 – 1566;,
Ether – Wikipedia,
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