Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 50868-73-0, name is 2-Methoxy-6-methylaniline, A new synthetic method of this compound is introduced below., Recommanded Product: 2-Methoxy-6-methylaniline
Examples 9 and 10 2 g of 1,2,3,4-Tetrafluoroanthraquinone and 25 g of 2-methoxy-6-methylaniline were charged in a 50 cc, four necked flask and then the reaction was carried out at 80C for about 4 hours.. After completion of reaction, 2-methoxy-6-methylaniline was distilled out from the reaction solution, and a column purification using a column with a silica gel was effected to give rise to 1.04 g of 2-(2-methoxy-6-methylanilino)-1,3,4-trifluoroanthraquinone (Reference Dye 7′) (yield 36.7 mol%) and 1.05 g of 2,3-bis(2-methoxy-6-methylanilino)-1,4-difluoroanthraquinone (Dye 8) (yield 28.6 mol%).. The physical properties of Reference Dye 7′ and analytical values defining the compound are tabulated in Table 2 and the physical properties of Dye 8 and analytical values defining the compound are tabulated in Table 3.
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; NIPPON SHOKUBAI CO., LTD.; EP833203; (2004); B1;,
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