Related Products of 589-10-6, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 589-10-6, name is (2-Bromoethoxy)benzene belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
General procedure: Chlorosulfonic acid (20.00 mmol) was added dropwise to an ice-salt bath solution of the appropriate bromoalkoxyphenyl (1-3) (10.00 mmol) dissolved in dichloromethane (25 ml) at -10 C. After stirring for 2 h, the reaction mixture was allowed to warm to room temperature, and was stirred for an additional hour. The reaction mixture was then poured into 200 g of cracked ice and extracted with dichloromethane. The organic layer was washed with brine, dried over anhydrous sodium sulfate and filtered. The solvent was removed under reduced pressure to afford the corresponding 4-(bromoalkoxy)benzenesulfonyl chloride derivatives (4-6).
The synthetic route of (2-Bromoethoxy)benzene has been constantly updated, and we look forward to future research findings.
Reference:
Article; Ceras, Javier; Cirauqui, Nuria; Perez-Silanes, Silvia; Aldana, Ignacio; Monge, Antonio; Galiano, Silvia; European Journal of Medicinal Chemistry; vol. 52; (2012); p. 1 – 13;,
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