Continuously updated synthesis method about 1,2-Bis(4-methoxyphenyl)ethyne

The synthetic route of 2132-62-9 has been constantly updated, and we look forward to future research findings.

2132-62-9, name is 1,2-Bis(4-methoxyphenyl)ethyne, belongs to ethers-buliding-blocks compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. HPLC of Formula: C16H14O2

take 1,2-dicarbonylmethyl ester-Indolizine 46.6mg (corresponding to 0.20 mmol), 71.5 mg (equivalent to 0.30 mmol) of 1,2-bis(4-methoxyphenyl) acetylene, 4.5 mg of palladium acetate (equivalent to 0.02 mmol), Potassium acetate was 5.0 mg (equivalent to 0.01 mmol), 1.5 ml of dimethylsulfoxide and then stirred under heating at 130 C for 1 hours under 1 atmosphere of oxygen and separated to obtain the sixth number target Product 78.9 mg (yield 84%).

The synthetic route of 2132-62-9 has been constantly updated, and we look forward to future research findings.