13353-03-2, name is 2,4,6,8-Tetraoxanonane, belongs to ethers-buliding-blocks compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. Application In Synthesis of 2,4,6,8-Tetraoxanonane
2.7 mol of dimethoxymethoxymethane, 0.5 mol of 2,6-methylethylaniline and 100 mLBenzene was added to the reaction flask and incubated at 75-80 C for 18 h.After the completion of the reaction, the methoxymethanol and benzene recovered were separated and separated.Distillation gives 2,6-methyl-N-(methoxymethoxymethyl)aniline,The yield was 97.2% and the content was 98.9%.The total yield of the above two steps was 93.51%.
The synthetic route of 13353-03-2 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Shandong Binnong Technology Co., Ltd.; Xu Jiajun; Sheng Qingquan; Zhang Jun; (7 pag.)CN110183334; (2019); A;,
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