Related Products of 2062-98-8,Some common heterocyclic compound, 2062-98-8, name is Perfluoro(2-methyl-3-oxahexanoyl) fluoride, molecular formula is C6F12O2, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
In the implementation of the example 1 on the basis of the, to amplify production test: the full the fluorine is positive n-propyl vinyl ether (PPVE) 1 kg, hexafluoropropylene oxide dimer 1.5 kg, cesium fluoride 120g and diethylene glycol dimethyl ether 2.6L adding 10L in the reactor, the temperature is increased to 95 C, stirring for 2 hours, the reaction pressure will not change the observation, cooling, opening the reaction kettle, separating out the lower liquid product distillation is C11 the re-compounding process 1.95 kg, yield is 87%.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route Perfluoro(2-methyl-3-oxahexanoyl) fluoride, its application will become more common.
Reference:
Patent; Tianjin Changlu Chemical New Material Co., Ltd; Zhang, Zhijun; Zhao, Xinghua; Xu, Yashuo; Wang, Bo; Xiao, Shan; (5 pag.)CN105503552; (2016); A;,
Ether – Wikipedia,
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