In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 39538-68-6, name is 2-Methoxy-4-methylaniline belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. Quality Control of 2-Methoxy-4-methylaniline
General procedure: To a magnetically-stirred, ice-bathed, solution of substituted aniline (1 equiv) in acetone (20 mL) at 0 C was added cyanuric chloride (1 equiv), and the resulting mixture was stirred at 0 C for 2 h and then at room temperature for an additional 2 h. Subsequently, crushed ice (10 mL) was added to the reaction, and the mixture was allowed to warm up to room temperature over 1 h. The solid was collected by vacuum filtration and was washed with water three times (3-10 mL).45
The synthetic route of 39538-68-6 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Shahin, Rand; Taha, Mutasem O.; Bioorganic and Medicinal Chemistry; vol. 20; 1; (2012); p. 377 – 400;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem