Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 768-70-7, name is 3-Ethynylanisole, This compound has unique chemical properties. The synthetic route is as follows., category: ethers-buliding-blocks
General procedure: In an oven-dried Schlenk tube 2-iodophenol 6 (0.5 mmol), terminalalkyne 4 (0.5 mmol), PdO/MWCNT (5 mol%), K2CO3(1 mmol) and solvent (DMSO) (1.0 mL) were added. Theresulting reaction mixture was stirred at 120 C for 24 h. Theprogress of the reaction was monitored by TLC. After completionof reaction, the reaction mixture was allowed to coolto room temperature, then diluted with (10 mL) ethyl acetateand NH4Cl (10 mL) was added fallowed by extraction withethyl acetate. The organic layers were dried (Na2SO4) andconcentrated in vacuum. Purification of the residue by silicagel column chromatography using petroleum ether/ethylacetate as the eluent furnished the benzofuran 7.
According to the analysis of related databases, 768-70-7, the application of this compound in the production field has become more and more popular.
Reference:
Article; Lakshminarayana, Bhairi; Mahendar, Lodi; Chakraborty, Jhonti; Satyanarayana, Gedu; Subrahmanyam, Ch; Journal of Chemical Sciences; vol. 130; 5; (2018);,
Ether – Wikipedia,
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