Application of 20265-97-8, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 20265-97-8, name is 4-Methoxyaniline hydrochloride belongs to ethers-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
General procedure: 4-methyl-4?-hydroxyazobenzene (Azo1). 6,8 g (0.05 mol) as hydrochloride was dissolvedin 100 mL hydrochloric acid (2M). Solution was cooled by ice bath up to0C and solution of 3,3 g (0.05 mol) sodium nitrite in minimal volume of water wasadded slowly. To the cooled solution of phenol 4,4 g (0.05 mol) in water the diazoniumsalt was added under stirring. Yellow azodye precipitate was filtered, washedby cooled water and dried. Substance purification was made by recrystallization fromisopropanol.
The synthetic route of 4-Methoxyaniline hydrochloride has been constantly updated, and we look forward to future research findings.
Reference:
Article; Tarasenko, Vitaliy; Nadtoka, Oksana; Syromyatnikov, Vladimir; Molecular Crystals and Liquid Crystals; vol. 590; 1; (2014); p. 97 – 104;,
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