Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 588-63-6, name is (3-Bromopropoxy)benzene, A new synthetic method of this compound is introduced below., name: (3-Bromopropoxy)benzene
The 148mg Na dissolved in 20ml of absolute ethanol until complete dissolution, 6-benzyl-2-thiouracil200mg (0.92mmol) and 1-(3-bromopropoxy)benzene 297mg (1.38mmol) was added, at room temperature after stirring overnight the reaction was complete by TLC; column chromatography, P:E = 5:1,2:1,1:1, finally give 257 mg of the product, as a white solid, a yield of 79.17percent
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; Peking University; Zhang, Liang; FU, YUHONG; Qin, Hua; Wang, Xiao Wei; Liu, Jun Yi; (30 pag.)CN103864699; (2016); B;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem