Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 1663-61-2, name is (Triethoxymethyl)benzene, A new synthetic method of this compound is introduced below., Recommanded Product: 1663-61-2
Phenyltriethoxymethane (0.5 mL) and acetic anhydride (0.94 mL) were added to malononitrile (0.17 g), and the mixture was stirred at 140 ° C. overnight.After the reaction solution was cooled to room temperature, the solvent was distilled off under reduced pressure to obtain a crude product.Purification by silica gel column chromatography (ethyl acetate – hexane)2- (Ethoxy (phenyl) methylene) malononitrile(Compound 0022-1, 334 mg) was obtained
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; FUJIFILM CORPORATION; KYOTO UNIVERSITY; KATO, TAKAYUKI; HIRAI, ATSUSHI; MATSUOKA, MASAO; SHIMURA, KAZUYA; (62 pag.)JP6052673; (2016); B2;,
Ether – Wikipedia,
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