Sources of common compounds: 7-Methoxy-2,3,4,5-tetrahydrobenzo[f][1,4]thiazepine

Statistics shows that 7-Methoxy-2,3,4,5-tetrahydrobenzo[f][1,4]thiazepine is playing an increasingly important role. we look forward to future research findings about 145903-31-7.

Related Products of 145903-31-7, These common heterocyclic compound, 145903-31-7, name is 7-Methoxy-2,3,4,5-tetrahydrobenzo[f][1,4]thiazepine, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

Novel compounds of this general structure were prepared by reacting 7-methoxy-2,3,4,5-tetrahydro-1,4-benzothiazepine (1) with triphosgene, in the presence of a base (Et3N), followed by addition of a primary or secondary amine or an alcohol. A representative synthesis of this general process is depicted in Scheme 6 below.

Statistics shows that 7-Methoxy-2,3,4,5-tetrahydrobenzo[f][1,4]thiazepine is playing an increasingly important role. we look forward to future research findings about 145903-31-7.

Reference:
Patent; Marks, Andrew R.; Landry, Donald W.; Deng, Shi Xian; Cheng, Zhen Zhuang; US2005/215540; (2005); A1;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem