Adding a certain compound to certain chemical reactions, such as: 70894-71-2, name is N-(4-Methoxybenzyl)cyclopropanamine, belongs to ethers-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 70894-71-2, category: ethers-buliding-blocks
General procedure: N-cyclopropyl-N-substituted benzylamine (4.0 mmol) inethanol was mixed with carbon disulfide (4.0 mmol) under ice coldcondition. To the resultant yellow dithiocarbamic acid solution,aqueous solution of NiCl2,6H2O (2.0 mmol) was added with constantstirring. The solid which precipitated was washed severaltimes with cold water and then dried (Fig. 1).
At the same time, in my other blogs, there are other synthetic methods of this type of compound, N-(4-Methoxybenzyl)cyclopropanamine, and friends who are interested can also refer to it.
Reference:
Article; Sathiyaraj; Srinivasan; Thirumaran; Velmurugan; Journal of Molecular Structure; vol. 1102; (2015); p. 203 – 209;,
Ether – Wikipedia,
Ether | (C2H5)2O – PubChem