Related Products of 588-63-6, These common heterocyclic compound, 588-63-6, name is (3-Bromopropoxy)benzene, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
General procedure: Maslinic acid (MA, 1equiv) was dissolved in dry DMF (5mL), and finely grounded potassium carbonate (5 equiv) was added. After 60min of stirring at room temperature, the corresponding alkyl or benzyl bromide (2equiv) was added, and stirring was continued for 18h. The mixture was poured into an ice cold aq. HCl (5percent, 50mL), and the white precipitate was filtered off. Chromatographic purification (silica gel, hexane/ethyl acetate, 7:3) and recrystallization (ethanol) afforded the product.
Statistics shows that (3-Bromopropoxy)benzene is playing an increasingly important role. we look forward to future research findings about 588-63-6.
Reference:
Article; Siewert, Bianka; Pianowski, Elke; Obernauer, Anja; Csuk, Rene?; Bioorganic and Medicinal Chemistry; vol. 22; 1; (2014); p. 594 – 615;,
Ether – Wikipedia,
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