Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 27060-75-9, name is 1-Bromo-4-methoxy-2-methylbenzene, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 27060-75-9
General procedure: An argon flushed pressure tube was charged with indole (59 mg, 0.5mmol), bromobenzene (62 muL, 0.5 mmol), Mo(CO)6 (132 mg, 0.5mmol), DBU (75 muL, 0.5 mmol), K3PO4 (106 mg, 0.5 mmol), Pd(OAc)2(3.4 mg, 3 mol%), BuPAd2 (10.8 mg, 6 mol%), and DMF (3 mL). The tubewas subsequently sealed and the mixture was stirred at 120 C for 16h. Afterwards, the reaction mixture was diluted with CH2Cl2 (3 × 5mL) and washed with H2O (3 × 5 mL). The aqueous layer was extractedwith CH2Cl2 (2 × 5 mL), the combined organic phases were dried(Na2SO4), and the solvent was evaporated. The crude product was purifiedby column chromatography (pentane-EtOAc (8:2) with additionof 0.5% Et3N) to give benzoylindole as a viscous oil that solidifiedon standing; yield: 98 mg (89%); mp 64-65 C.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 27060-75-9.
Reference:
Article; Wu, Xiao-Feng; Oschatz, Stefan; Sharif, Muhammad; Langer, Peter; Synthesis; vol. 47; 17; (2015); p. 2641 – 2646;,
Ether – Wikipedia,
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